Organometallic chemistry, Volume 27 by M. Green
By M. Green
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Extra resources for Organometallic chemistry, Volume 27
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P. Spaniol, and J. Okuda, Organometallics, 1997,16,4765. J. Karl, G. Erker, and R. Frohlich, J. Am. Chem. , 1997, 119, I 1165. J. Karl and G. Erker, Chem. -Recueil, 1997,130, 1261. J. Karl, G. Erker, and R. Frohlich, J. Organornet. , 1997,535, 59. G. Rodriguez and G. C. Bazan, J. Am. Chem. ,1997,119,343. G. J. Pindado, M. ThorntonPett, and M. Bochmann, Chem. , 1997,609. G. J. Pindado, M. ThorntonPett, and M. Bochmann, J. Chem. , 1997,3115. G. G. Lavoie and R. G. Bergman, Angew. , Int. Ed. , 1997,36,2450.
The alkylation of [CI-P-B~'-~~~~X[~]-(OM~) with LiPh led to a dimeric dimetallic aryl compound, [(pL-p-Bu'-calix(OMe)(0)3}2Zr2Ph2] 18, where the calixarene unit bridges two metal atoms and the methoxy groups are only weakly bound to the metal. The spectator methoxy group binds strongly to the metal in the monomeric q2-iminoacyl [pBu'-calix-(OMe)(0)3Zr(BuN'=CPh)] , formed from the migratory insertion of BuNC' into the Zr-Ph bond. Six of the proposed structures in the paper have been supported by X-ray crystallography.